HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-Nonanol, 9-bromo- → 14-Methyl-1-pentadecanol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-Nonanol, 9-bromo- | HCID 108700 | — |
| Reactant | 1-Bromo-5-methylhexane | HCID 520726 | — |
| Product | 14-Methyl-1-pentadecanol | HCID 5283265 | 55% |
Reaction Steps
14-methylpentadecan-1-ol was prepared from 9-bromononanol and 5-methylhexylbromide in 55% yield. The 1H NMR and MS-ESI data matched those reported by Yuasa et al. (Yuasa and Tsuruta (2004) Flavour and Fragrance Journal 19:199-204).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07994143B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-85af44fe06d44b07baca65b45c22147f |
| Source note | uspto-grants-2011_08 |