HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 15986279, compound → HCID 15986353, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 15986279 | HCID 15986279 | — |
| Reactant | HCID 178418361 | HCID 178418361 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 15986353 | HCID 15986353 | 100.4% |
Reaction Steps
A solution of 2-vinyl-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one from Example 10 (40 mg, 0.17 mmol) and 5 mg of palladium on charcoal (10%) in 50 ml of methanol was stirred under 1 atm of hydrogen for 70 min. Filtration and evaporation to dryness afforded the title compound as a pale yellow solid (41 mg, 87%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07994160B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-f95200d4c2f14bf1a155fec1bc71e50f |
| Source note | uspto-grants-2011_08 |