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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1670403Generated: October 30, 2026

HCID 15986279, compound → HCID 15986353, compound

https://huagongshe.com/reaction/1670403

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 15986279HCID 15986279—
ReactantHCID 178418361HCID 178418361—
CatalystPalladiumHCID 23938—
SolventMethanolHCID 887—
ProductHCID 15986353HCID 15986353100.4%

Reaction Steps

A solution of 2-vinyl-5,10-dihydro-3,4,5,10-tetraaza-dibenzo[a,d]cyclohepten-11-one from Example 10 (40 mg, 0.17 mmol) and 5 mg of palladium on charcoal (10%) in 50 ml of methanol was stirred under 1 atm of hydrogen for 70 min. Filtration and evaporation to dryness afforded the title compound as a pale yellow solid (41 mg, 87%).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07994160B2
Source datasetuspto-grants-2011_08
ORD IDord-f95200d4c2f14bf1a155fec1bc71e50f
Source noteuspto-grants-2011_08