反应详情

100 mg of 32 (390 μmol), 113 mg of 38 (390 μmol) and 162 mg of sodium 2-ethylhexanoate (0.98 mmol) in 2 mL of THF are successively introduced into a Wheaton tube, with stirring and under an argon atmosphere. The stirring is maintained at RT for 24 h. The reaction medium is concentrated to dryness. The residues are chromatographed on a silica cartridge (8 g, eluent AcOEt). 79 mg of expected product Ex16 are recovered.

1. concentrationThe reaction medium is concentrated to dryness
2. customThe residues are chromatographed on a silica cartridge (8 g, eluent AcOEt)
3. custom79 mg of expected product Ex16 are recovered