L-Tartaric acid → HCID 86623708, compound

Participants

Reaction Steps

Dissolve 7-chloro-6-(2-methyl-3H-imidazol-4-ylthiomethyl)-2,3,4,5-tetrahydro-1H-benzo[d]azepine (193 mg, 0.63 mmol) in methanol (12 mL) and water (1 mL) and add L-(+)-tartaric acid (94 mg, 0.63 mmol). Stir the mixture for 1 h and concentrate the mixture in vacuo. Dissolve in water, and freeze dry the solution to provide the title compound (32 mg, 100%). MS (APCI) m/z: 308 (M+H)+.

Provenance & Evidence