Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Potassium Iodide | HCID 4875 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 3,5-Dibromo-4-Hydroxybenzaldehyde | HCID 18100 | — |
| Reactant | 3-Methoxybenzyl bromide | HCID 4067207 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 86633608 | HCID 86633608 | — |
Reaction Steps
A mixture of 3,5-dibromo-4-hydroxybenzaldehyde (0.28 g), 1-bromomethyl-3-methoxybenzene (0.15 mL), potassium carbonate (0.29 g) and potassium iodide (42 mg) in 10 mL absolute ethanol was stirred at 80° C. for 2 days. The reaction mixture was concentrated and the title compound was obtained as a off-white solid after flash column chromatography (silica gel, heptane/ethyl acetate (3/7, v/v)), Rf=0.51).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07994189B2 |
|---|
| Source dataset | uspto-grants-2011_08 |
|---|
| ORD ID | ord-9f201f560d184d6b9aaa95d91b1106c8 |
|---|
| Source note | uspto-grants-2011_08 |
|---|
