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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1670811Generated: October 26, 2026

3-Phenyloxolan-2-one → 3-Cyclohexyl-dihydro-furan-2-one

https://huagongshe.com/reaction/1670811

Reaction equation

Participants

RoleNameHCIDCharge
Reactant3-Phenyloxolan-2-oneHCID 23269—
CatalystRhodiumHCID 23948—
SolventEthanolHCID 702—
Product3-Cyclohexyl-dihydro-furan-2-oneHCID 2201323492.1%

Reaction Steps

Stir a mixture of 3-phenyl-dihydro-furan-2-one (9.0 g), rhodium on carbone (5%, 3.62 g) and ethanol (220 mL) on a hydrogenation parr shaker at 60 psi, 60° C. for 18 hours. Remove the reaction from the parr shaker and filter the mixture through celite, concentrate the filtrate to afford 8.6 g (92%) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07994176B2
Source datasetuspto-grants-2011_08
ORD IDord-1b2ddf76b64c4c319bb096b1f34f8ec6
Source noteuspto-grants-2011_08