HRID1670811

反应详情

EQUATION

反应方程式

HRID 1670811 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

Stir a mixture of 3-phenyl-dihydro-furan-2-one (9.0 g), rhodium on carbone (5%, 3.62 g) and ethanol (220 mL) on a hydrogenation parr shaker at 60 psi, 60° C. for 18 hours. Remove the reaction from the parr shaker and filter the mixture through celite, concentrate the filtrate to afford 8.6 g (92%) of the title compound.

WORKUP

后处理

  1. customRemove
  2. customthe reaction from the parr shaker
  3. filtrationfilter the mixture through celite
  4. concentrationconcentrate the filtrate