HRID1670855

反应详情

EQUATION

反应方程式

HRID 1670855 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

To a round bottom flask, 380 mg (0.957 mmol) of 3 was dissolved in 3 mL of methanol. To this solution 3 mL of 4 N HCl in dioxane was added slowly, stirred at room temperature for 1 h and concentrated to afford a quantitative amount (354 mg) of 4.

WORKUP

后处理

  1. concentrationconcentrated