HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → Diethylaminoethylaniline dihydrochloride
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | 1,2-Ethanediamine, N1,N1-diethyl-N2-phenyl- | HCID 74271 | — |
| Solvent | Methanol | HCID 887 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | Diethylaminoethylaniline dihydrochloride | HCID 56729931 | — |
Reaction Steps
To a round bottom flask, 62.6 mg (0.153 mmol) of 5 was dissolved in 1 mL of methanol. To this solution 1 mL of 4 N HCl in dioxane was added slowly, stirred at room temperature for 1 h and concentrated to afford a quantitative amount (52.7 mg) of 6.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07994172B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-82f9d4801e924a9eb76a9a08a30de5b8 |
| Source note | uspto-grants-2011_08 |