HRID1671480

反应详情

EQUATION

反应方程式

HRID 1671480 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

2

PROCEDURE

实验过程

A suspension of (2S)-2-(4-fluorophenyl)-4-(benzyl)morpholine (250 mg) and 5% Pd—C (0.106 g) in ethanol (5 mL) was treated with hydrogen for 1 hr at 33-35° C. The suspension was filtered through celite and washed with ethanol. The solvent was evaporated to give (2S)-2-(4-fluorophenyl)morpholine (160 mg, 94%) as a white solid.

WORKUP

后处理

  1. filtrationThe suspension was filtered through celite
  2. washwashed with ethanol
  3. customThe solvent was evaporated