HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl bromoacetate → HCID 43401322, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl bromoacetate | HCID 7748 | — |
| Reactant | 2-(3-Fluorophenyl)ethanamine | HCID 533928 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 43401322 | HCID 43401322 | — |
Reaction Steps
Ethyl bromoacetate (0.166 g, 0.11 mL, 0.001 mol) and 3-fluorophenethylamine (0.139 g, 0.13 mL, 0.001 mol) were stirred in MeOH (10 mL) for 48 h. The solvent was removed in vacuo, and the residue was purified by column chromatography (silica gel, hexanes:EtOAc=2:3) to generate VIII-3 (0.083 g, 37%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07994326B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-5fa875f6ef154138a2bb2694452085ab |
| Source note | uspto-grants-2011_08 |