HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1671755Generated: November 3, 2026
Hydrochloric Acid → HCID 178484818, compound
https://huagongshe.com/reaction/1671755
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 178501225 | HCID 178501225 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 178484818 | HCID 178484818 | 47.5% |
Reaction Steps
A mixture of methyl cis-4-[{[(1,1-dimethylethyl)oxy]carbonyl}(methyl)amino]cyclohexanecarboxylate (˜10 g, crude product from above) and 1M HCl in dioxane (20 mL) was heated to 50° C. and allowed to stir overnight. The mixture was concentrated to give the 3 g of crude product. MS (ES+): m/e 172.1 [M+H]+.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| Patent number | US07994317B2 |
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| Source dataset | uspto-grants-2011_08 |
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| ORD ID | ord-a6b20da3e5864e3c8382e18b299dd11a |
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| Source note | uspto-grants-2011_08 |
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