HuagongsheHuagongshe Chemistry Print Report · For research reference only
Piperidine → 1-Butylpiperidine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Piperidine | HCID 8082 | — |
| Reactant | Butyl iodide | HCID 10962 | — |
| Solvent | Diethyl Ether | HCID 3283 | — |
| Product | 1-Butylpiperidine | HCID 78654 | — |
Reaction Steps
45.0 g piperidine (0.53 mol) was added to 150 g ethyl ether. 48.6 g iodobutane (0.26 mol) was then added drop wise. After 3 days the resulting piperidine hydroiodide salt was removed by filtration and the N-butylpiperidine was recovered from the ether solution.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07998457B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-e7b70704628b4aacb51b4e3d59fbfa76 |
| Source note | uspto-grants-2011_08 |