HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethylformamide dimethyl acetal → HCID 54387791, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethylformamide dimethyl acetal | HCID 78373 | — |
| Reactant | 2-Aminoimidazole | HCID 82140 | — |
| Product | HCID 54387791 | HCID 54387791 | — |
Reaction Steps
To the crude 2-aminoimidazole (18.2 g) was added dimethylformamide dimethyl acetal (145 mL) (Aldrich) and stirred at room temperature overnight. The reagent was removed in vacuo to give crude 2 (32.66 g) which was taken on to the next step (tritylation) without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07998462B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-3a17c757b1bc4c66ae78780072034265 |
| Source note | uspto-grants-2011_08 |