2-(Methylamino)ethanol → HCID 85830820, compound

Participants

Reaction Steps

50 Parts by weight of 28% sodium methylate is added to 100 parts by weight of methyl stearate and 26 parts by weight of N-methylethanolamine, and an amidation reaction is allowed to proceed at 90° C. while removing methanol. Subsequently, sodium methylate is decomposed by using 66 parts by weight of 35% hydrochloric acid and after dehydration, sodium chloride is removed by filtration. Thereafter, 33 parts by weight of stearic acid is added to 100 parts by weight of the solid material, and an esterification reaction is performed at 170° C. while effecting dehydration, whereby N-stearoyl-N-methylamino-ethyl stearate is obtained.

Provenance & Evidence