참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetic Anhydride | HCID 7918 | — |
| 반응물 | 3-Methyl-2-oxaspiro[4.5]decan-1-ol | HCID 59649210 | — |
| 용매 | Pyridine | HCID 1049 | — |
| 생성물 | 3-Methyl-2-oxaspiro[4.5]decan-1-yl acetate | HCID 59649211 | — |
반응 단계
A mixture of 11 g of 3-methyl-2-oxaspiro[4.5]decan-1-ol, 7.7 g of pyridine and 9.2 g of acetic anhydride was heated at 50° C. for 12 hours. The reaction mixture was concentrated. The concentrate was purified by distillation, obtaining 13 g (yield 960) of the target compound, 3-methyl-2-oxaspiro[4.5]decan-1-yl acetate.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US07998657B2 |
|---|
| 출처 데이터셋 | uspto-grants-2011_08 |
|---|
| ORD ID | ord-6af6488394e749faadde0d6633899e39 |
|---|
| 출처 메모 | uspto-grants-2011_08 |
|---|
