HRID1672117

反应详情

EQUATION

反应方程式

HRID 1672117 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

The following are introduced into a 25 ml round-bottomed flask, in order: 11-(1-pyrrolyl)undecan-1-oic acid (2 mmol; 503 mg), of N-hydroxysulphosuccinimide (2 mmol; 434 mg) and dicyclohexylcarbodiimide (DCC) (2.4 mmol; 495 mg). 10 ml of dimethylformamide (DMF) are subsequently added. A cloudy mixture is obtained, which is subjected to magnetic stirring overnight.

WORKUP

后处理

  1. additionThe following are introduced into a 25 ml round-bottomed flask, in order
  2. customA cloudy mixture is obtained