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Dicyclohexylcarbodiimide → Sulfo-n-hydroxysulfosuccinimide
関与物質
| 役割 | 名称 | HCID | 仕込み量 |
|---|---|---|---|
| 反応物 | Dicyclohexylcarbodiimide | HCID 10868 | — |
| 反応物 | N-Hydroxysulfosuccinimide | HCID 133909 | — |
| 反応物 | 11-Pyrrol-1-yl-undecanoic acid | HCID 67349574 | — |
| 溶媒 | Dimethylformamide | HCID 6228 | — |
| 生成物 | Sulfo-n-hydroxysulfosuccinimide | HCID 11254355 | — |
反応手順
The following are introduced into a 25 ml round-bottomed flask, in order: 11-(1-pyrrolyl)undecan-1-oic acid (2 mmol; 503 mg), of N-hydroxysulphosuccinimide (2 mmol; 434 mg) and dicyclohexylcarbodiimide (DCC) (2.4 mmol; 495 mg). 10 ml of dimethylformamide (DMF) are subsequently added. A cloudy mixture is obtained, which is subjected to magnetic stirring overnight.
情報源と証拠
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 特許番号 | US07998726B2 |
| 出典データセット | uspto-grants-2011_08 |
| ORD ID | ord-a380c7e186dc4840827cf64bcae7c453 |
| 出典メモ | uspto-grants-2011_08 |