HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromoaniline → HCID 60046925, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromoaniline | HCID 11992 | — |
| Reactant | HCID 60046927 | HCID 60046927 | — |
| Solvent | Acetic Acid | HCID 176 | — |
| Product | HCID 60046925 | HCID 60046925 | — |
Reaction Steps
The title compound is prepared in analogy to Example 19d, starting from 0.5 g (1.756 mmol) 4-chloro-3-nitro-6-phenyl-quinoline (Example 53d) and 0.339 g (1.932 mmol) 2-bromoaniline in 3 ml acetic acid. mp: 198-204° C.; MS: 420 (M++1); HPLC: tret=12.17 min (Grad 1).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07998972B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-89dfaf65b0cd431989bbc98e79103f00 |
| Source note | uspto-grants-2011_08 |