HCID 24759086, compound → HCID 67355797, compound

Participants

Reaction Steps

5-Benzyl-N-cyclohexyl-5-azaspiro[2.4]heptane-6-carboxamide (prepared according to Example 30, 14 mg, 0.0000448 mol) was dissolved in methanol (1 mL). To this solution was added Pd/C (3 mg) and the resulting mixture was stirred under an atmosphere of hydrogen overnight. The catalyst was filtered off and the volatiles were removed in vacuo to afford the desired product (10.3 mg), which was used in the next step without further purification. LC/MS: 223.2 (M+H)+.

Provenance & Evidence