Hydrochloric Acid → HCID 67337734, compound

HRID 1672511Notes

Reaction equation

HRID 1672511 reaction equation
[Br-].[F:2][CH2:3][CH2:4][N+:5]1[CH:13]=[C:12]2[N:7](C(=O)[NH:9][CH2:10][CH2:11]2)[CH:6]=1.[ClH:15]>>[ClH:15].[ClH:15].[F:2][CH2:3][CH2:4][N:5]1[CH:13]=[C:12]([CH2:11][CH2:10][NH2:9])[N:7]=[CH:6]1

Participants

3

Reactant 2

HCID 313Hydrochloric AcidHCID 86634503HCID 86634503, compound

Product 1

HCID 67337734HCID 67337734, compound

Procedure

A solution of 2-(2-Fluoro-ethyl)-5-oxo-5,6,7,8-tetrahydro-imidazo[1,5-c]pyrimidin-2-ium bromide (0.64 g, 2.42 mmol) in aqueous 6 M HCl, was heated at 130° C. for 60 hours and the solvent evaporated to yield the titled product.

Workup

  1. customthe solvent evaporated

Sources & evidence

ORD record
ord-91a899df1fa84d58a810f037c456ccf4
Source dataset
uspto-grants-2011_08
Patent number
US07998990B2

Reaction notes

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