HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → Trifluoroacetate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 86634504 | HCID 86634504 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | Trifluoroacetate | HCID 84468 | — |
| Product | HCID 86634505 | HCID 86634505 | — |
Reaction Steps
A solution of [2-(2-Fluoro-ethylcarbamoyl)-ethyl]-carbamic acid tert-butyl ester (0.353 g, 1.51 mmol) in dichloromethane (10 ml) was treated with trifluoroacetic acid (1 ml) and the reaction stirred at ambient temperature for 4 hours. The solvent was evaporated to dryness to yield the titled product as a trifluoroacetate salt.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07998990B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-ab087be44230416e9fbd43799d91d375 |
| Source note | uspto-grants-2011_08 |