HuagongsheHuagongshe Chemistry Print Report · For research reference only
Phosphine, triphenyl-, hydrobromide → HCID 86634295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Phosphine, triphenyl-, hydrobromide | HCID 517696 | — |
| Reactant | 2-(Trifluoromethoxy)benzyl alcohol | HCID 2777245 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 86634295 | HCID 86634295 | — |
Reaction Steps
5 g (26 mmol) of 2-trifluoromethoxybenzyl alcohol and 8.5 g (24.7 mmol) of triphenylphosphonium bromide are heated under reflux in 100 ml of acetonitrile for 3 h. After cooling, the resulting precipitate is filtered off with suction and dried. 13.5 g (quant.) of the title compound are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07998988B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-db768cf2be984f8b9180cc9667863dea |
| Source note | uspto-grants-2011_08 |