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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1673093Generated: October 31, 2026

HCID 59715735, compound → HCID 59715643, compound

https://huagongshe.com/reaction/1673093

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 59715735HCID 59715735—
CatalystHCID 178418390HCID 178418390—
SolventTetrahydrofuranHCID 8028—
ProductHCID 59715643HCID 5971564310.4%

Reaction Steps

Palladium-carbon (10%, 5.0 mg) was added to a solution of the compound of Example B158 (2.0 mg) in tetrahydrofuran (2.0 ml), and the mixture was stirred at room temperature under nitrogen atmosphere (1 atm) for 1 hour. The catalyst was removed by filtration, and the filtrate was concentrated. The residue was purified by silica gel column chromatography to give the title compound (0.21 mg).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07999090B2
Source datasetuspto-grants-2011_08
ORD IDord-2086269127d94cba9c2110c2f096df7c
Source noteuspto-grants-2011_08