HCID 178448029, compound → HCID 178455757, compound

Participants

Reaction Conditions

Reaction Steps

4-(trans-4-(trans-4-Propylcyclohexyl)cyclohexyl)-2-oxetanone (1 g, 3.1 mmol) obtained in Example 2 was placed in a reactor, the interior of which was then sufficiently replaced by nitrogen. The reactor was heated, and after heating to 170° C. for 3 hours, it was cooled to room temperature. The resulting solid was dissolved in heptane and purified with silica gel chromatography to provide trans-1-ethenyl-4-(trans-4-propyl-cyclohexyl)cyclohexane (0.83 g, 30 mmol, yield: 95%).

Provenance & Evidence