HCID 178444496, compound → HCID 178455759, compound

Participants

Reaction Conditions

Reaction Steps

4-(trans-4-(trans-4-pentylcyclohexyl)cyclohexyl) -2-oxetanone obtained in Example 5 was placed in a reactor, the interior of which was then sufficiently replaced by nitrogen. The reactor was heated, and after heating to 170° C. for 3 hours, it was cooled to room temperature. The resulting solid was dissolved in heptane and purified with silica gel chromatography to provide trans-1-ethenyl -4-(trans-4-pentylcyclohexyl)-cyclohexane at a yield of 95%.

Provenance & Evidence