HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 67023921, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 24993725 | HCID 24993725 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 67023921 | HCID 67023921 | — |
Reaction Steps
To a solution of Example 315 (200 mg, 0.36 mmol) in 5.0 mL of CH2Cl2 was added 500 μL of TFA. After stirring at rt for 16 h, the reaction mixture was concentrated. The amine TFA salt was taken onto next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999107B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-15dc5dd305c24edc8d3394d0934a740a |
| Source note | uspto-grants-2011_08 |