HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine hydrate (1:1) → HCID 67020069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine hydrate (1:1) | HCID 24654 | — |
| Reactant | HCID 67329693 | HCID 67329693 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 67020069 | HCID 67020069 | — |
Reaction Steps
A solution of the product of Step B (22 mmol) and 2.0 mL of hydrazine hydrate in 10 mL of CH3OH was refluxed for 10 h. After cooling to rt, the reaction mixture was concentrated to give the product, which was taken into the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999107B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-9c5d0b42ecbd41c283698378a1537c3f |
| Source note | uspto-grants-2011_08 |