HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 86622727, compound → HCID 67020004, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 86622727 | HCID 86622727 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 67020004 | HCID 67020004 | — |
Reaction Steps
A solution of the product of Step A (364 mg, 0.64 mmol) in 10 mL of 20% TFA in CH2Cl2 was stirred at rt for 2 h. The reaction mixture was concentrated to give the product, which was used in the next step without further purification.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999107B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-d63484ccd2cf418998ce0e04e50901f1 |
| Source note | uspto-grants-2011_08 |