HCID 67344515, compound → HCID 67344440, compound

Participants

Reaction Steps

70 mg of 5% palladium-carbon was added to 4 mL of ethyl acetate solution containing 0.35 g of 2-nitro-4-(4-phenyl-1-butenyl)benzoate and stirred under hydrogen atmosphere at room temperature for 8 hours. Insoluble were removed by filtration, and the solvent was evaporated under reduced pressure to obtain 0.40 g of tert-butyl 2-amino-4-(4-phenylbutyl)benzoate as yellow oil.

Provenance & Evidence