Methanol → HCID 57879481, compound

Participants

Reaction Steps

20 mg of 5% palladium-carbon was added to a mixed solution of 1 mL of methanol and 2 mL of ethyl acetate containing 0.10 g of 2-(benzamido)-4-((E)-2-phenylvinyl)benzoic acid and stirred under hydrogen atmosphere at room temperature for 5 hours. Insoluble were removed by filtration and the solvent was evaporated under reduced pressure. Hexane and diisopropyl ether were added to the obtained residue and a solid substance was separated by filtration to obtain 69 mg of 2-(benzamido)-4-phenethylbenzoic acid as white solid.

Provenance & Evidence