Trifluoroacetic acid → HCID 11552505, compound

HRID 1673383Notes

Reaction equation

HRID 1673383 reaction equation
FC(F)(F)C(O)=O.[C:8]([NH:16][C:17]1[CH:29]=[C:28]([CH2:30][CH2:31][CH2:32][CH2:33][C:34]2[CH:39]=[CH:38][CH:37]=[CH:36][CH:35]=2)[CH:27]=[CH:26][C:18]=1[C:19]([O:21]C(C)(C)C)=[O:20])(=[O:15])[C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1>>[C:8]([NH:16][C:17]1[CH:29]=[C:28]([CH2:30][CH2:31][CH2:32][CH2:33][C:34]2[CH:35]=[CH:36][CH:37]=[CH:38][CH:39]=2)[CH:27]=[CH:26][C:18]=1[C:19]([OH:21])=[O:20])(=[O:15])[C:9]1[CH:10]=[CH:11][CH:12]=[CH:13][CH:14]=1

Participants

3

Reactant 2

HCID 6422Trifluoroacetic acidHCID 67342408HCID 67342408, compound

Product 1

HCID 11552505HCID 11552505, compound

Procedure

4.9 mL solution of trifluoroacetic acid containing 0.50 g of tert-butyl 2-(benzamido)-4-(4-phenylbutyl)benzoate was stirred at room temperature for 2 hours and 30 minutes. A solid substance was separated by filtration to obtain 0.16 g of 2-(benzamido)-4-(4-phenylbutyl)benzoic acid as white solid.

Workup

  1. customA solid substance was separated by filtration

Sources & evidence

ORD record
ord-e2b84e8dde8044ec9f11902003799029
Source dataset
uspto-grants-2011_08
Patent number
US07999132B2

Reaction notes

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