HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → Benzoic Acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | 2-(benzamido)-4-((E)-2-(3-methoxyphenyl)vinyl)benzoic acid | HCID 57879424 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | Benzoic Acid | HCID 243 | — |
Reaction Steps
1.0 mL of methanol, 2.0 mL of ethyl acetate and 2.0 mg of 5% palladium-carbon were added to the obtained 2-(benzamido)-4-((E)-2-(3-methoxyphenyl)vinyl)benzoic acid and stirred under hydrogen atmosphere at room temperature for 2 hours. Insoluble were removed by filtration, and the solvent was evaporated under reduced pressure to obtain 6.3 mg of 2-(benzamido)-4-(2-3-methoxyphenyl)ethyl)benzoic acid as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999132B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-058d08704eb642b3a9c7650d9f77e25d |
| Source note | uspto-grants-2011_08 |