Methanol → HCID 57879409, compound

Participants

Reaction Steps

30 mg of 5% palladium-carbon was added to a mixed solution of 1.5 mL of methanol and 2 mL of ethyl acetate containing the obtained 0.15 g of 2-(benzamido)-4-benzoylbenzoic acid and stirred under hydrogen atmosphere at room temperature for ten hours. Insoluble were removed by filtration and the solvent was evaporated under reduced pressure. Hexane was added to the obtained residue and a solid substance was separated by filtration to obtain 0.11 g of 2-(benzamido)-4-benzylbenzoic acid as white solid.

Provenance & Evidence