Methanol → HCID 67342385, compound

Participants

Reaction Steps

0.51 mL of 2.0 mol/b aqueous sodium hydroxide was added dropwise to a mixed solution of 3 mL of methanol and 3 mL of tetrahydrofuran containing 0.31 g of methyl 2-(benzamido)-4-(phenoxymethyl)benzoate while ice-cooled and stirred an room temperature for 5 hours and 30 minutes, the solvent was evaporated under reduced pressure and water was added and pH was adjusted to pH 4.0 with 1.0 mol/L hydrochloric acid. A solid substance was separated by filtration to obtain 0.21 g of 2-(benzamido)-1-(phenoxymethyl)benzoic acid as white solid.

Provenance & Evidence