HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 57879342, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 67341418 | HCID 67341418 | — |
| Product | HCID 57879342 | HCID 57879342 | 81.6% |
Reaction Steps
3.0 mL of trifluoroacetic acid suspension containing 0.17 g of tert-butyl 2-(benzamido)-4-((E)-2-(2-hydroxyphenyl)vinyl)benzoate was stirred at room temperature for 30 minutes. The solvent was evaporated under reduced pressure, toluene was added, and the solvent was evaporated under reduced pressure. Hexane was added to the obtained residue and a solid substance was separated by filtration to obtain 0.12 g of 2-(benzamido)-4-((E)-2-(2-hydroxyphenyl)vinyl)benzoic acid as yellow solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999132B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-0cc13d4743594cd3807686b0a6ea2d28 |
| Source note | uspto-grants-2011_08 |