HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67342390, compound → HCID 57879361, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67342390 | HCID 67342390 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 57879361 | HCID 57879361 | — |
Reaction Steps
10 mL of trifluoroacetic acid was added to the obtained tert-butyl 2-(4-fluorobenzamido)-4-((E)-2-(3-methoxyphenyl)vinyl)benzoate and stirred at room temperature for 2 hours. The solvent was evaporated under reduced pressure and diisopropyl ether was added to the obtained residue and a solid substance was separated by filtration to obtain 45 mg of 2-(4-fluorobenzamido)-4-((E)-2-(3-methoxyphenyl)vinyl)benzoic acid as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999132B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-329e8a4afa804b04bbdbb23082b2abc0 |
| Source note | uspto-grants-2011_08 |