HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanol → HCID 57879585, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 57879386 | HCID 57879386 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57879585 | HCID 57879585 | — |
Reaction Steps
7.6 mg of potassium carbonate was added to a mixed solution of 0.5 mL of methanol and 0.5 mL of tetrahydrofuran containing 15 mg of 2-(4-acetoxybenzamido)-4-(3-chlorophenyl)benzoic acid and stirred at room temperature for 2 hours. After insoluble were removed by filtration, 10% citric acid aqueous solution was added and a solid substance was separated by filtration to obtain 10 mg of 4-(3-chlorophenyl)-2-(4-hydroxybenzamido)benzoic acid as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999132B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-bf1586531d9f454f8204b17b92a5cb35 |
| Source note | uspto-grants-2011_08 |