HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 67343462, compound → HCID 57879500, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 67343462 | HCID 67343462 | — |
| Solvent | Trifluoroacetic acid | HCID 6422 | — |
| Product | HCID 57879500 | HCID 57879500 | — |
Reaction Steps
10 mL of trifluoroacetic acid was added to the obtained tert-butyl 2-((E)-3-(3,4-dimethoxyphenyl)acrylamido)-4-phenoxybenzoate and stirred at room temperature for 2 hours. The solvent was evaporated under reduced pressure, and diisopropyl ether was add to the obtained residue, and a solid substance was separated by filtration to obtain 13 mg of (E)-2-(3-(3,4-dimethoxyphenyl)acrylamido)-4-phenoxybenzoic acid as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999132B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-4791818de02c42bda241ce03b757affb |
| Source note | uspto-grants-2011_08 |