HuagongsheHuagongshe Chemistry Print Report · For research reference only
Citric Acid → HCID 57879535, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Citric Acid | HCID 311 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 57879462 | HCID 57879462 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57879535 | HCID 57879535 | 90.1% |
Reaction Steps
0.50 mL of methanol, 0.50 mL of tetrahydrofuran and 8.3 mg of potassium carbonate were added to 15 mg of 2-(3-acetoxybenzamido)-4-phenylbenzoic acid at room temperature sequentially and stirred at the same temperature for 2 hours. 10% citric acid aqueous solution was added to the reaction mixture and a solid substance was separated by filtration to obtain 12 mg of 2-(3-hydroxybenzamido)-4-phenylbenzoic acid as while solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999132B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-5a54ca2c9e2248b0880afbe90fa0259e |
| Source note | uspto-grants-2011_08 |