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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1673507Generated: October 31, 2026

Citric Acid → HCID 57879544, compound

https://huagongshe.com/reaction/1673507

Reaction equation

Participants

RoleNameHCIDCharge
ReactantCitric AcidHCID 311—
ReactantMethanolHCID 887—
ReactantPotassium CarbonateHCID 11430—
ReactantHCID 57879340HCID 57879340—
SolventTetrahydrofuranHCID 8028—
ProductHCID 57879544HCID 5787954461.6%

Reaction Steps

0.50 mL of methanol, 0.50 mL of tetrahydrofuran and 4.2 mg of potassium carbonate were added sequentially to 8.0 mg of 2-(3-acetoxybenzamido)-4-phenoxybenzoic acid at room temperature and stirred at the same temperature for 2 hours. 10% citric acid aqueous solution was added to the reaction mixture and a solid substance was separated by filtration to obtain 4.4 mg of 2-(3-hydroxybenzamido)-4-phenoxybenzoic acid as whine solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07999132B2
Source datasetuspto-grants-2011_08
ORD IDord-49b31cb3d2fe46fe824f64e144b0522d
Source noteuspto-grants-2011_08