HuagongsheHuagongshe Chemistry Print Report · For research reference only
Citric Acid → HCID 57879544, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Citric Acid | HCID 311 | — |
| Reactant | Methanol | HCID 887 | — |
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | HCID 57879340 | HCID 57879340 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 57879544 | HCID 57879544 | 61.6% |
Reaction Steps
0.50 mL of methanol, 0.50 mL of tetrahydrofuran and 4.2 mg of potassium carbonate were added sequentially to 8.0 mg of 2-(3-acetoxybenzamido)-4-phenoxybenzoic acid at room temperature and stirred at the same temperature for 2 hours. 10% citric acid aqueous solution was added to the reaction mixture and a solid substance was separated by filtration to obtain 4.4 mg of 2-(3-hydroxybenzamido)-4-phenoxybenzoic acid as whine solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07999132B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-49b31cb3d2fe46fe824f64e144b0522d |
| Source note | uspto-grants-2011_08 |