Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 57879392 | HCID 57879392 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 57879299 | HCID 57879299 | 108.6% |
Reaction Steps
3.0 mL of methanol, 2.0 mL of ethyl acetate and 4.0 mg of 5% palladium-carbon were added to 20 mg of 2-(4-nitrobenzamido)-4-phenoxybenzoic acid at room temperature and stirred under hydrogen atmosphere at 40° C. for 8 hours. Insoluble were removed by filtration, and the solvent was evaporated under reduced pressure to obtain 20 mg of 2-(4-aminobenzamido)-4-phenoxybenzoic acid as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07999132B2 |
|---|
| Source dataset | uspto-grants-2011_08 |
|---|
| ORD ID | ord-b8604bb665814ca88761d8a291876095 |
|---|
| Source note | uspto-grants-2011_08 |
|---|
