Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Methanol | HCID 887 | — |
| Reactant | HCID 57879597 | HCID 57879597 | — |
| Catalyst | HCID 178418390 | HCID 178418390 | — |
| Solvent | Ethyl Acetate | HCID 8857 | — |
| Product | HCID 57879350 | HCID 57879350 | 37.1% |
Reaction Steps
2.0 mL of methanol, 2.0 mL of ethyl acetate and 3.0 mg of 5% palladium-carbon were added to 15 mg of 2-(3-nitrobenzamido)-4-phenylbenzoic acid at room temperature and stirred under hydrogen atmosphere at 40° C. for 2 hours. Insoluble were removed by filtration, and the solvent was evaporated under reduced pressure to obtain 5.1 mg of 2-(3-aminobenzamido)-4-phenylbenzoic acid as white solid.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US07999132B2 |
|---|
| Source dataset | uspto-grants-2011_08 |
|---|
| ORD ID | ord-f3eab499951947ada0efdc7d87783bb4 |
|---|
| Source note | uspto-grants-2011_08 |
|---|
