Methanol → HCID 67343432, compound

Participants

Reaction Steps

10 mg of 5% palladium-carbon was added to a mixed solution of 4.0 mL of methanol and 8.0 mL of ethyl acetate containing 50 mg of tert-butyl 2-(benzamido)-4-(2-nitroanilino)benzoate and stirred under hydrogen atmosphere at room temperature for 1 hour and 30 minutes. After insoluble were removed by filtration, the solvent was evaporated under reduced pressure to obtain 46 mg of tert-butyl 4-(2-aminoanilino)-2-(benzamido)benzoate as pale yellow solid.

Provenance & Evidence