HRID1673519

反应详情

EQUATION

反应方程式

HRID 1673519 的结构方程式

PROCEDURE

实验过程

5.0 mL of trifluoroacetic acid was added to the obtained tert-butyl 2-(benzamido)-4-(3-chloro-4-Methylphenyl)benzoate and stirred at room temperature for 2 hours. The solvent was evaporated under reduced pressure and methanol was added to the obtained residue and a solid substance was separated by filtration to obtain 14 mg of 2-(benzamido)-4-(3-chloro-4-methylphenyl)benzoic acid as white solid.

WORKUP

后处理

  1. customThe solvent was evaporated under reduced pressure and methanol
  2. additionwas added to the obtained residue
  3. customa solid substance was separated by filtration