Back
HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1673542Generated: October 31, 2026

Trifluoroacetic acid → HCID 57879326, compound

https://huagongshe.com/reaction/1673542

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 67344183HCID 67344183—
SolventDichloromethaneHCID 6344—
ProductHCID 57879326HCID 5787932657.8%

Reaction Steps

0.5 mL of trifluoroacetic acid was added to 0.5 mL of methylene chloride solution containing 10 mg of tert-butyl 2-(3-cyanobenzamido)-4-phenoxybenzoate and stirred at room temperature for 2 hours. The solvent was evaporated under reduced pressure and diisopropyl ether was added to the obtained residue and a solid substance was separated by filtration to obtain 5.0 mg of 2-(3-cyanobenzamido)-4-phenoxybenzoic acid as white solid.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS07999132B2
Source datasetuspto-grants-2011_08
ORD IDord-114d2fe4f90e4aea9d8dcf727cd05ddf
Source noteuspto-grants-2011_08