Hydrochloric Acid → HCID 57879550, compound

Participants

Reaction Steps

0.16 mL of 2.0 mol/L aqueous sodium hydroxide was added to a mixed solution of 1.0 mL of methanol and 1.0 mL of tetrahydrofuran containing 0.10 g of methyl 2-(benzamido)-4-(3-chlorophenoxy)benzoate while ice-cooled and stirred at room temperature for 5 hours. The reaction mixture was added to water and 1.0 mol/L hydrochloric acid while ice-cooled, and a solid substance was separated by filtration to obtain 92 mg of 2-(benzamido)-4-(3-chlorophenoxy)benzoic acid as white solid.

Provenance & Evidence