HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Aminophenol → 6-ethyl-N,N'-bis(3-hydroxyphenyl)-1,3,5-triazine-2,4-diamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Aminophenol | HCID 11568 | — |
| Reactant | 2,4-Dichloro-6-ethyl-1,3,5-triazine | HCID 12776 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | 6-ethyl-N,N'-bis(3-hydroxyphenyl)-1,3,5-triazine-2,4-diamine | HCID 9858379 | — |
Reaction Steps
After dissolving 3-aminophenol (2.18 g, 20 mmol) in 1,4-dioxane (20.0 mL), 2,4-dichloro-6-ethyl-1,3,5-triazine (1.78 g, 10 mmol) was added and stirring carried out for 3 hours at 100° C. under a nitrogen atmosphere.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003645B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-0a8da5e126084112bde0de5c025ceca9 |
| Source note | uspto-grants-2011_08 |