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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 1674508Generated: October 30, 2026

Glycol monoethyl ether → HCID 23031993, compound

https://huagongshe.com/reaction/1674508

Reaction equation

Participants

RoleNameHCIDCharge
ReactantGlycol monoethyl etherHCID 8076—
Reactant3-MethoxyanilineHCID 10824—
ReactantHCID 23031990HCID 23031990—
ProductHCID 23031993HCID 23031993—

Reaction Conditions

Temperature130 °C

Reaction Steps

2-methyl-4-chloro-6-(3-hydroxyphenylamino)pyrimidine (0.71 g, 3.0 mmol) was added to a 2-ethoxyethanol (2.0 mL) solution of 3-methoxyaniline (0.37 g, 3.0 mmol) under a nitrogen atmosphere and the reaction mixture stirred for 5 hours at 130° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08003645B2
Source datasetuspto-grants-2011_08
ORD IDord-f2d1ed1ada71430685038dbc0d2d47d5
Source noteuspto-grants-2011_08