HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 57511295, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | Triethylsilane | HCID 12052 | — |
| Reactant | HCID 67338427 | HCID 67338427 | — |
| Solvent | Dichloromethane | HCID 6344 | — |
| Product | HCID 57511295 | HCID 57511295 | — |
Reaction Steps
To a solution of [(2-chloro-5-dimethylamino-phenyl)-(3,4-dimethoxy-benzenesulfonyl)-amino]-acetic acid tert-butylester (1.160 g) in dry DCM (5.5 mL) were added successively triethylsilane (0.423 mL) and TFA (4.8 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08003654B2 |
| Source dataset | uspto-grants-2011_08 |
| ORD ID | ord-ca1263811a34496284e24bfe16dce42b |
| Source note | uspto-grants-2011_08 |